Issue 35

R. Konečná et alii, Frattura ed Integrità Strutturale, 35 (2016) 31-40; DOI: 10.3221/IGF-ESIS.36.04 38 a) K a = 1.6 MPam 1/2 , da/dN ~ 10 -7 mm/cycle. b) K a = 5.0 MPam 1/2 , da/dN ~ 10 -5 mm/cycle. Figure 12 : Fracture profiles of fatigue crack path, LM Discussion SLM Inconel 718 in contrast to conventionally manufactured alloy exhibits strong features of local directional solidification. The SLM CT specimens exhibit a columnar microstructure [12] which was found and analyzed also in this paper (Fig. 5, Fig. 6). Microstructure of parallel elongated fine columns (Fig. 6a, c) was characterized in [13, 14] as a fine columnar microdendritic structure. The sections of fine columns by a metallographic plane inclined at a high angle to their long axis have an ellipsoidal shape (Fig. 6c, Fig. 7f) whose dimensions are obviously dependent on the mutual orientation of columns and the metallographic section. The cuboidal structure corresponds to the γ ʹ phase (precipitates Ni 3 (Al, Ti). The preferred formation of γ ʹ rather than γ ʹʹ precipitation has been shown to be dependent on Ti + Al/Nb ratio [4, 5]. Cozar et al. [5] conclude that if the Ti + Al/Nb ratio is above a critical value (from 0.9 to 1) the γ ʹ precipitates formation prevails over the γ ʹʹ formation. That ratio for the present material is 1.26 that is substantially higher than the critical range. In some cases special cube-shaped γ ʹ particles coated with a γ ʹʹ shell were identified. This effect is related to very slow coarsening rate [5]. The propagation of long cracks in conventionally manufactured Inconel 718 at ambient and high temperatures was studied intensively in the past [15-17], because this alloy is often used for fabrication of components exposed to long term cyclic loading at high temperatures. Also the mechanism of the crack growth was a subject of investigation. The threshold values for propagation of long cracks have been shown to be dependent on temperature and microstructure. Recently Yamada et al. [18] presented a detailed study on the effect of crack closure on the crack growth. Their measurements indicate high threshold at R = 0.1, which is attributed to anticipated crack closure in the loading cycle. The near-threshold FCG data at R = 0.7, on the other hand, are apparently crack closure free. The fatigue crack growth curves, particularly in the threshold region, were shown to be strongly dependent on the chemical composition. The content of boron ranging from 12 to 100 ppm decreases the crack growth rate substantially [19]. The loading with the stress intensity factor amplitude K a = 5.0 MPam 1/2 in the case of the lowest B concentration results in identical crack growth rate of 1 x 10 -6 mm/cycle as in material with highest B content loaded at K a = 7.2 MPam 1/2 [19]. Contrary to the case of conventionally manufactured alloy the knowledge on the mechanical properties of SLM Inconel 718 is limited. As regards the tensile properties, they are comparable to those of wrought material [20]. Influence of processing parameters, like atmosphere in the building chamber, was reported, but these effects seem to be weak. On the other hand, the comparison of the fatigue crack growth curves of wrought and SLM manufactured alloy shows substantial differences, Fig. 13. The data determined in this study are compared with the measurements by Clavel and Pineau [15]. Both crack growth experiments were performed for identical loading asymmetry R = 0.1 on similar CT specimens. The crack growth rates above 5 x 10 -5 mm/cycle in both materials can be considered as identical within the data scatter band. Strong difference, however, appears in the near-threshold region. The resistance of the SLM material against crack growth is substantially lower. Similar conclusions can be made when data for SLM material are compared with result by Yuen et al. [17]. The threshold stress intensity factor amplitude K ath of SLM material based on the crack growth rate 1 x 10 -7 mm/cycle makes only 25 % of the value determined in [15] and 35 % of value found in [17]. The threshold value in conventionally manufactured Inconel has been shown to depend on the boron content. In our case the boron content is higher than 100 ppm. It means that the threshold value determined in this study for SLM material should be compared with the value of about K ath ~ 6 MPam 1/2 [19]. This comparison again indicates the disadvantage of SLM produced material as regards the resistance to the growth of long cracks. The explanation of the lower threshold values of SLM alloy can be substantiated by the different microstructure. The SLM alloy exhibits very fine grain. The grain size is of about 10  m, whereas the alloy studied by Clavel and Pineau [15] had the grain size 30  m. This finding is consistent with general trend of decreasing threshold with decreasing grain size. The fracture profile presented in Fig. 12a shows that the fatigue crack propagates in the threshold region through the microstructure